Sodium Sulfite → Sodium cycloheptylmethanesulfonate

反応式

Br[CH2:2][CH:3]1[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.[S:10]([O-:13])([O-:12])=[O:11].[Na+:14].[Na+]>>[CH:3]1([CH2:2][S:10]([O-:13])(=[O:12])=[O:11])[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.[Na+:14]

参加物

反応物 2

HCID 24437Sodium Sulfite

HCID 23000753(Bromomethyl)cycloheptane

生成物 1

HCID 23670189Sodium cycloheptylmethanesulfonate

実験手順

The subtitle compound was prepared by the method of Preparation 61 from 1-(bromomethyl)cycloheptane [Preparation 66] and sodium sulfite. The crude product was purified by recrystallisation from water to afford sodium cycloheptylmethanesulfonate as a white solid.

後処理

customThe crude product was purified by recrystallisation from water

出典と根拠

ORDレコード: ord-492a299d80e24777a8278b20b341f235
出典データセット: uspto-grants-2003_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06610707B1

反応ノート

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