Methylamine → n-Methyl-3-nitropyridin-4-amine
反応式
CO[C:3]1[CH:8]=[CH:7][N:6]=[CH:5][C:4]=1[N+:9]([O-:11])=[O:10].[CH3:12][NH2:13]>C(O)C>[CH3:12][NH:13][C:3]1[CH:8]=[CH:7][N:6]=[CH:5][C:4]=1[N+:9]([O-:11])=[O:10]参加物
4
実験手順
2.36 g 4-methoxy-3-nitro-pyridine and 2.33 ml methylamine (40% in water) are refluxed in 25 ml of ethanol for 3 h. Then the reaction mixture is evaporated to dryness. 2.3 g product are obtained as a solid.
後処理
- customThen the reaction mixture is evaporated to dryness
出典と根拠
- ORDレコード
- ord-35e601a38c5e47dfb5ec3c8613cdef1f
- 出典データセット
- uspto-grants-2014_06
- 特許番号
- US08754073B2
反応ノート
読み込み中…