反応式
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][Si:13](Cl)(Cl)Cl.C1(C)C=CC=CC=1>CCCCCCCCCCCCCCCC>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][SiH3:13]参加物
4
反応条件
- 温度
- 60 °C
実験手順
Freshly cleaned slides were immersed in a solution of bromoundecyl-trichlorosilane (3% v/v) in hexadecane or toluene. The reaction was heated to 60° C. for 4-6 hours then allowed to cool to room temperature. The slides were washed with CH2Cl2 and ethanol then blown dry under a stream of argon, producing a film with an advancing water contact angle of 82±2 degrees above horizontal.
後処理
- temperatureto cool to room temperature
- washThe slides were washed with CH2Cl2 and ethanol
- customthen blown dry under a stream of argon
- customproducing a film with an advancing water contact angle of 82±2 degrees above horizontal
出典と根拠
- ORDレコード
- ord-7d1aa318407a44748ba2e762b5c1f179
- 出典データセット
- uspto-grants-2014_06
- 特許番号
- US08759008B2
関連ノート
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