関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | (11-Bromoundecyl)trichlorosilane | HCID 15895053 | — |
| 溶媒 | Hexadecane | HCID 11006 | — |
| 生成物 | 11-Bromoundecylsilane | HCID 57350085 | — |
反応手順
Freshly cleaned slides were immersed in a solution of bromoundecyl-trichlorosilane (3% v/v) in hexadecane or toluene. The reaction was heated to 60° C. for 4-6 hours then allowed to cool to room temperature. The slides were washed with CH2Cl2 and ethanol then blown dry under a stream of argon, producing a film with an advancing water contact angle of 82±2 degrees above horizontal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08759008B2 |
|---|
| 出典データセット | uspto-grants-2014_06 |
|---|
| ORD ID | ord-7d1aa318407a44748ba2e762b5c1f179 |
|---|
| 出典メモ | uspto-grants-2014_06 |
|---|
