反应详情

温度

60 °C

Freshly cleaned slides were immersed in a solution of bromoundecyl-trichlorosilane (3% v/v) in hexadecane or toluene. The reaction was heated to 60° C. for 4-6 hours then allowed to cool to room temperature. The slides were washed with CH2Cl2 and ethanol then blown dry under a stream of argon, producing a film with an advancing water contact angle of 82±2 degrees above horizontal.

1. temperatureto cool to room temperature
2. washThe slides were washed with CH2Cl2 and ethanol
3. customthen blown dry under a stream of argon
4. customproducing a film with an advancing water contact angle of 82±2 degrees above horizontal