64910-48-1 → 4-Amino-3-(methylamino)benzonitrile

HRID 410949ノート

反応式

HRID 410949 の反応式
[CH3:1][NH:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][C:10]=1[N+:11]([O-])=O)[C:6]#[N:7]>[Pd]>[NH2:11][C:10]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][C:3]=1[NH:2][CH3:1]

参加物

3

反応物 1

HCID 1101939864910-48-1

生成物 1

HCID 110080674-Amino-3-(methylamino)benzonitrile収率 0.1%

試薬・触媒・溶媒 1

HCID 23938Palladium触媒

実験手順

4-Amino-3-methylamino-benzonitrile (1.17 mg) was prepared by following General Procedure B starting from 3-methylamino-4-nitro-benzonitrile (1.33 g) and Pd/C (10% by weight, 133 mg). The crude product was used in the next step without further purification.

後処理

  1. customThe crude product was used in the next step without further purification

出典と根拠

ORDレコード
ord-d79cc169abc14c7ba5ba7ed911ad189e
出典データセット
uspto-grants-2014_06
特許番号
US08759535B2

反応ノート

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