HCID 67333354、化合物 → HCID 67332947、化合物
反応式
[CH3:1][NH:2][C:3]1[CH:4]=[C:5]([CH2:12][C:13]([NH2:15])=[O:14])[CH:6]=[CH:7][C:8]=1[N+:9]([O-])=O>CO.CCOC(C)=O.[Pd]>[NH2:9][C:8]1[CH:7]=[CH:6][C:5]([CH2:12][C:13]([NH2:15])=[O:14])=[CH:4][C:3]=1[NH:2][CH3:1]参加物
4
実験手順
2-(4-Amino-3-methylamino-phenyl)-acetamide (554 mg) was prepared by following General Procedure B beginning with 2-(3-methylamino-4-nitro-phenyl)-acetamide (727.0 mg) and Pd/C (20% by weight, 140.0 mg) in MeOH:EtOAc (1:1, 10.0 mL). The crude product was used in the next step without further purification.
後処理
- customThe crude product was used in the next step without further purification
出典と根拠
- ORDレコード
- ord-2e542e1202a349398ecf85aebc979c50
- 出典データセット
- uspto-grants-2014_06
- 特許番号
- US08759535B2
反応ノート
読み込み中…