Thionyl Chloride → 4-(Methylamino)-3-nitrobenzoyl chloride

HRID 411049

反応式

HRID 411049 の反応式
[CH3:1][NH:2][C:3]1[CH:11]=[CH:10][C:6]([C:7](O)=[O:8])=[CH:5][C:4]=1[N+:12]([O-:14])=[O:13].S(Cl)([Cl:17])=O>>[CH3:1][NH:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([Cl:17])=[O:8])=[CH:5][C:4]=1[N+:12]([O-:14])=[O:13]

参加物

3

反応物 2

HCID 24386Thionyl ChlorideHCID 2834754-(Methylamino)-3-nitrobenzoic acid

生成物 1

HCID 179464494-(Methylamino)-3-nitrobenzoyl chloride

反応条件

温度
80 °C

実験手順

4-Methylamino-3-nitro-benzoyl chloride (4.3 g) was prepared starting from 4-methylamino-3-nitro-benzoic acid (4 g) in thionyl chloride (20 mL). The reaction was heated to 80° C. for 8 h. The solvent was evaporated to isolate pure compound without any further purification.

後処理

  1. customThe solvent was evaporated
  2. customto isolate pure compound
  3. customwithout any further purification

出典と根拠

ORDレコード
ord-cf67af8299fd443997516bc33d342552
出典データセット
uspto-grants-2014_06
特許番号
US08759535B2

関連ノート

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