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Acetic Anhydride → 1-Acetyl-7-methylindoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | 7-Methyl-2,3-dihydro-1H-indole | HCID 12377788 | — |
| 生成物 | 1-Acetyl-7-methylindoline | HCID 14361366 | — |
反応手順
A solution of 7-methylindoline (10.2 g) in acetic anhydride (25 ml) was refluxed for 30 min. After cooling, the reaction solution was poured into ice water (250 ml) and the resulting crystal was filtered by means of suction, heated and vacuum dried to yield the end product (11.7 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06559149B1 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-532146205184410b96c1b186bb23c4a5 |
| 出典メモ | uspto-grants-2003_05 |