Water → Laurolactam

HRID 41343

反応式

HRID 41343 の反応式
[C:1]1(=[N:13]O)[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[OH2:15]>>[C:1]1(=[O:15])[NH:13][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]1

参加物

3

反応物 2

HCID 962WaterHCID 136762Cyclododecanone, oxime

生成物 1

HCID 13690Laurolactam

実験手順

For example, after the reaction of cyclododecanone oxime, the reaction can be worked up by adding water, extracting a product with an organic solvent and then evaporating the solvent to give laurolactam, which can be further separated and purified by, for example, distillation or crystallization.

後処理

  1. customthe reaction
  2. extractionextracting a product with an organic solvent
  3. customevaporating the solvent

出典と根拠

ORDレコード
ord-bf9970b51c7248ce8751f7ff38820cf3
出典データセット
uspto-grants-2013_09
特許番号
US08530645B2

関連ノート

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