反応式
[S:1].[CH2:2]1[CH:6]2[C@@H:7]3[CH:11]=[CH:10][C@H:9]([CH:5]2[CH:4]=[CH:3]1)[CH2:8]3.C(=O)([O-])[O-].[Ca+2]>O>[S:1].[CH2:2]1[CH:6]2[C@@H:7]3[CH:11]=[CH:10][C@H:9]([CH:5]2[CH:4]=[CH:3]1)[CH2:8]3参加物
5
反応条件
- 温度
- 150 °C
実験手順
Into a 4 liter autoclave were placed 425 g of sulfur, 75 g of DCPD, 2500 ml of water and 20 g of calcium carbonate. The reactor was then sealed and heated to 150° C. for three hours with stirring. After cooling to ambient temperature, the sulfur/DCPD adduct was isolated as small beads.
後処理
- customThe reactor was then sealed
- temperatureAfter cooling to ambient temperature
出典と根拠
- ORDレコード
- ord-0005c5c1607a4f3f973b1472511c893f
- 出典データセット
- uspto-grants-1988_12
- 特許番号
- US04792589
関連ノート
読み込み中…