Trifluoromethanesulfonic acid → 2-Ethylimidazolium trifluoromethanesulfonate

HRID 41840

反応式

HRID 41840 の反応式
[CH2:1]([C:3]1[NH:4][CH:5]=[CH:6][N:7]=1)[CH3:2].[F:8][C:9]([F:15])([F:14])[S:10]([OH:13])(=[O:12])=[O:11]>O>[F:8][C:9]([F:15])([F:14])[S:10]([O-:13])(=[O:12])=[O:11].[CH2:1]([C:3]1[NH:7][CH:6]=[CH:5][NH+:4]=1)[CH3:2]

参加物

4

反応物 2

HCID 62406Trifluoromethanesulfonic acidHCID 661302-Ethylimidazole

生成物 1

HCID 1317293002-Ethylimidazolium trifluoromethanesulfonate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

2-ethylimidazole was solved with distilled water, in which an equimolar amount of trifluoromethanesulfonic acid was dropped and stirred while being cooled. The reaction product was predried at 100° C. and then vacuum-dried at 120° C., thus obtaining a target ionic conductor.

後処理

  1. additionwas dropped
  2. temperaturewhile being cooled
  3. customwas predried at 100° C.
  4. customvacuum-dried at 120° C.
  5. customthus obtaining a target ionic conductor

出典と根拠

ORDレコード
ord-a842590af6784b67b66671dd9621b6d5
出典データセット
uspto-grants-2013_09
特許番号
US08535849B2

関連ノート

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