Sodium Hydroxide → 27457-28-9

HRID 418884ノート

反応式

HRID 418884 の反応式
Br[CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[S:10]([OH:13])(=[O:12])=[O:11].[OH-].[Na+:15]>>[CH2:2]=[CH:3][C:4]1[C:5]([S:10]([O-:13])(=[O:12])=[O:11])=[CH:6][CH:7]=[CH:8][CH:9]=1.[Na+:15]

参加物

3

反応物 2

HCID 14798Sodium HydroxideHCID 54404796HCID 54404796、化合物

生成物 1

HCID 2367857827457-28-9

実験手順

Next, 2-(2-bromoethyl)benzenesulfonic acid (10 g) was slowly added dropwise to a 1-mol/L aqueous solution of sodium hydroxide (100 mL), and the whole was stirred for 1 hour at room temperature. After that, the resultant was refluxed for 4 hours, and was then subjected to a dehydrobromination reaction, whereby sodium o-styrenesulfonate was obtained.

後処理

  1. temperatureAfter that, the resultant was refluxed for 4 hours
  2. customwas then subjected to a dehydrobromination reaction

出典と根拠

ORDレコード
ord-01f1bb2e32544311b86bd0d0a0ab4ba2
出典データセット
uspto-grants-2012_01
特許番号
US08093342B2

反応ノート

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