Sodium Hydroxide → Sodium 4-ethenylnaphthalenesulfonate
反応式
Br[CH2:2][CH2:3][C:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:7]([S:14]([OH:17])(=[O:16])=[O:15])=[CH:6][CH:5]=1.[OH-].[Na+:19]>>[CH:3]([C:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:7]([S:14]([O-:17])(=[O:15])=[O:16])=[CH:6][CH:5]=1)=[CH2:2].[Na+:19]参加物
3
実験手順
Next, 4-(2-bromoethyl)naphthalenesulfonic acid (10 g) was slowly added dropwise to a 1-mol/L aqueous solution of sodium hydroxide (100 mL), and the whole was stirred for 1 hour at room temperature. After that, the resultant was refluxed for 6 hours, and was then subjected to a dehydrobromination reaction, whereby sodium 4-ethenylnaphthalenesulfonate was obtained.
後処理
- temperatureAfter that, the resultant was refluxed for 6 hours
- customwas then subjected to a dehydrobromination reaction
出典と根拠
- ORDレコード
- ord-2ac93d6b7a6e4713af8aa13ce7509ead
- 出典データセット
- uspto-grants-2012_01
- 特許番号
- US08093342B2
反応ノート
読み込み中…