反応式
[Br:1][CH2:2][CH2:3][C:4]1[CH:13]=[CH:12][C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=1.[S:14](=O)(=[O:17])([OH:16])[OH:15]>>[Br:1][CH2:2][CH2:3][C:4]1[CH:13]=[CH:12][C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5]=1[S:14]([OH:17])(=[O:16])=[O:15]参加物
3
反応条件
- 温度
- 0 °C
実験手順
2-(2-bromoethyl)naphthalene (120 g) was stirred in an ice bath while fuming sulfuric acid (50 g) was slowly added dropwise. After the dropwise addition, the mixture was stirred at 0° C. for 30 hours, whereby 2-(2-bromoethyl)naphthalenesulfonic acid and a plurality of isomers were obtained, and then separated and purified.
後処理
- additionwas slowly added dropwise
- additionAfter the dropwise addition
出典と根拠
- ORDレコード
- ord-ebce4216be1f4dd7b193824955a78eba
- 出典データセット
- uspto-grants-2012_01
- 特許番号
- US08093342B2
関連ノート
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