化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Anhydride → Phenol, 3-bromo-, 1-acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 3-Bromophenol | HCID 11563 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Phenol, 3-bromo-, 1-acetate | HCID 141946 | — |
反応手順
3-bromophenol was dissolved in dichloromethane. Triethylamine (1 eq) and acetic anhydride (2 eq) were added and the mixture was stirred at room temperature for 5 hours. The solvent was eliminated by vacuum evaporation. The evaporation residue was taken up in dichloromethane then dried on magnesium sulfate. The solvent was eliminated by vacuum evaporation.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08106097B2 |
| 出典データセット | uspto-grants-2012_01 |
| ORD ID | ord-89e702bc6c0441768c9874858355db04 |
| 出典メモ | uspto-grants-2012_01 |