HRID425106

反应详情

EQUATION

反应方程式

HRID 425106 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

3-bromophenol was dissolved in dichloromethane. Triethylamine (1 eq) and acetic anhydride (2 eq) were added and the mixture was stirred at room temperature for 5 hours. The solvent was eliminated by vacuum evaporation. The evaporation residue was taken up in dichloromethane then dried on magnesium sulfate. The solvent was eliminated by vacuum evaporation.

WORKUP

后处理

  1. customThe solvent was eliminated by vacuum evaporation
  2. customthen dried on magnesium sulfate
  3. customThe solvent was eliminated by vacuum evaporation