反応式
[CH2:1]=[C:2]([CH3:4])[CH3:3].C(O)CCCCC.N#N.[C:14]([O:18]CCCCCC)([CH3:17])([CH3:16])[CH3:15]>>[C:2]([O:18][C:14]([CH3:17])([CH3:16])[CH3:15])([CH3:4])([CH3:3])[CH3:1]参加物
5
実験手順
300 mmoles of i-butene, 100 mmoles of 1-hexanol and 2.5 g of Ti-Si-catalyst powder are stirred in a 100 ml autoclave at a pressure of 40 bar N2 and a temperature of 150° C. over a period of 17 h. 17% of n-hexanol were converted into hexyl t-butyl ether with a selectivity of 90%.
出典と根拠
- ORDレコード
- ord-1b0b00f84d034ff3beb242a6e2c2856b
- 出典データセット
- uspto-grants-2001_11
- 特許番号
- US06319876B1
関連ノート
読み込み中…