HCID 54549583、化合物 → HCID 10107954、化合物
反応式
[C:1]([O:5][C:6]([C:8]1[S:9][C:10]([CH:13]=[CH:14][C:15]([O:17][CH2:18][CH3:19])=[O:16])=[CH:11][CH:12]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[H][H]>C(O)C.[Pd]>[C:1]([O:5][C:6]([C:8]1[S:9][C:10]([CH2:13][CH2:14][C:15]([O:17][CH2:18][CH3:19])=[O:16])=[CH:11][CH:12]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2]参加物
5
実験手順
0.846 g (3 mmol) of the product obtained in step d) were dissolved in 100 ml of dry ethanol. 150 mg of 10% palladium on charcoal were added, and the suspension was hydrogenated at 50° C. and 4 bar hydrogen pressure. After filtration the solvent was removed in vacuo. 0.6 g of a colourless oil were obtained.
後処理
- customwas hydrogenated at 50° C.
- filtrationAfter filtration the solvent
- customwas removed in vacuo
出典と根拠
- ORDレコード
- ord-074d49f404c746369c7bdb1fda0e1ba2
- 出典データセット
- uspto-grants-2003_12
- 特許番号
- US06660728B2
反応ノート
読み込み中…