L-Lysine → zinc L-lysinate

HRID 434180

反応式

HRID 434180 の反応式
[OH-].[Zn+2:2].[OH-].[NH2:4][C@H:5]([C:11]([OH:13])=[O:12])[CH2:6][CH2:7][CH2:8][CH2:9][NH2:10]>C(O)C>[NH2:4][C@H:5]([C:11]([O-:13])=[O:12])[CH2:6][CH2:7][CH2:8][CH2:9][NH2:10].[Zn+2:2].[NH2:4][C@H:5]([C:11]([O-:13])=[O:12])[CH2:6][CH2:7][CH2:8][CH2:9][NH2:10]

参加物

4

反応物 2

HCID 5962L-LysineHCID 9812759Zinc Hydroxide

生成物 1

HCID 14772515zinc L-lysinate

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

The zinc hydroxide precipitate was then placed into a beaker provided with a reflux condenser and 29.2 grams (0.2 Mole) of lysine was added. 100 ml ethanol was then added to this mixture and stirred and boiled at atmospheric pressure for 3 hours. The reaction mixture was then cooled and filtered yielding 35.5 grams of zinc lysinate in the form of a fine white powder.

後処理

  1. customprovided with a reflux condenser
  2. temperatureThe reaction mixture was then cooled
  3. filtrationfiltered

出典と根拠

ORDレコード
ord-b33e53b53fb846f7b8d7efa033c89018
出典データセット
uspto-grants-2003_12
特許番号
US06670494B1

関連ノート

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