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Water → 1,2-Benzisothiazolin-3-one manganese(II)chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Benzisothiazole | HCID 9225 | — |
| 反応物 | Manganese(2+) dichloride | HCID 10313134 | — |
| 生成物 | 1,2-Benzisothiazolin-3-one manganese(II)chloride | HCID 70534353 | 77% |
反応手順
To a solution of 1.26 g (0.01 mol) of anhydrous manganese chloride was added 4.5 g (0.03 mol) of 1,2-benzisothiazolin in 30 ml of water. The solution was concentrated to give a tan colored solid. The solid was thoroughly washed with dry acetone, filtered and dried at room temperature to yield 3.47 g (77%) of product, m.p. >250° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04396413 |
| 出典データセット | uspto-grants-1983_08 |
| ORD ID | ord-84bd98aad1874bdc9666e692682b4234 |
| 出典メモ | uspto-grants-1983_08 |