化工社化工社 化学情報印刷レポート · 研究参考用
Phenylacetone → 1-Phenyl-2-propanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenylacetone | HCID 7678 | — |
| 反応物 | Sodium borohydride | HCID 4311764 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 1-Phenyl-2-propanol | HCID 94185 | 86.7% |
反応手順
Sodium borohydride (10.0 g) was added portionwise to an ice cold stirred solution of 1-phenylpropan-2-one (30.0 g) in methanol (500 ml). The mixture was stirred for 4 hours, evaporated and partitioned between water (100 ml) and chloroform (200 ml). The organic phase was dried (MgSO4) and evaporated to give the product as a colourless oil (26.4 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04396627 |
| 出典データセット | uspto-grants-1983_08 |
| ORD ID | ord-e0ce0ce0e0664f128aefe1478c6790fe |
| 出典メモ | uspto-grants-1983_08 |