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HRID 434370作成日:2026年10月26日

Phenylacetone → 1-Phenyl-2-propanol

https://huagongshe.com/reaction/434370

反応式

関与物質

役割名称HCID仕込み量
反応物PhenylacetoneHCID 7678—
反応物Sodium borohydrideHCID 4311764—
溶媒MethanolHCID 887—
生成物1-Phenyl-2-propanolHCID 9418586.7%

反応手順

Sodium borohydride (10.0 g) was added portionwise to an ice cold stirred solution of 1-phenylpropan-2-one (30.0 g) in methanol (500 ml). The mixture was stirred for 4 hours, evaporated and partitioned between water (100 ml) and chloroform (200 ml). The organic phase was dried (MgSO4) and evaporated to give the product as a colourless oil (26.4 g).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04396627
出典データセットuspto-grants-1983_08
ORD IDord-e0ce0ce0e0664f128aefe1478c6790fe
出典メモuspto-grants-1983_08