Sodium Hydroxide → 1-(4-Acetylphenyl) propan-2-ol
反応式
C([O:4][CH:5]([CH3:16])[CH2:6][C:7]1[CH:12]=[CH:11][C:10]([C:13](=[O:15])[CH3:14])=[CH:9][CH:8]=1)(=O)C.[OH-].[Na+]>>[C:13]([C:10]1[CH:11]=[CH:12][C:7]([CH2:6][CH:5]([OH:4])[CH3:16])=[CH:8][CH:9]=1)(=[O:15])[CH3:14]参加物
3
実験手順
2-Acetoxy-1-(4-acetylphenyl) propane (4.5 g) was heated for 2 hours in refluxing 2 N sodium hydroxide solution. The mixture was allowed to cool and the product was extracted into ether. Evaporation of the dried (MgSO4) extracts gave an oil (3.8 g).
後処理
- temperatureto cool
- extractionthe product was extracted into ether
- customEvaporation of the
- dry with materialdried (MgSO4)
出典と根拠
- ORDレコード
- ord-f3d02f20e0444b7eb09a5c9a270b63d0
- 出典データセット
- uspto-grants-1983_08
- 特許番号
- US04396627
反応ノート
読み込み中…