反応式
B(O)(O)O.[CH2:5]([OH:19])[C@@H:6]([OH:18])[C@@H:7]([OH:17])[C@H:8]([OH:16])[C@@H:9]([OH:15])[C@@H:10]([OH:14])[C:11]([O-:13])=[O:12].[Na+]>O>[CH2:5]([OH:19])[C@@H:6]([OH:18])[C@@H:7]([OH:17])[C@H:8]([OH:16])[C@@H:9]([OH:15])[C@@H:10]([OH:14])[C:11]([OH:13])=[O:12]参加物
4
反応条件
- 温度
- 25 °C
実験手順
The diboron ester of glucoheptonic acid was prepared as follows: Approximately 124 grams (2 mols) of boric acid and 248 grams (1 mol) of sodium glucoheptonate were charged to an esterification vessel containing about 600 milliliters of water as a solvent. With stirring, the temperature was maintained at about 25° C. for approximately 30 minutes. The mixture was thereafter diluted to a final volume of one liter with additional water.
出典と根拠
- ORDレコード
- ord-14aa05a9e70445bf9970977a891a1384
- 出典データセット
- uspto-grants-1983_08
- 特許番号
- US04397812
関連ノート
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