反応式
[CH2:1]1[C:6](=O)[N:5](Cl)[C:3](=O)[CH2:2]1.[F:9][C:10]([F:22])([F:21])C(C1(CC)SCCCS1)=O.[CH3:23][O:24][CH:25]([O:28][CH3:29])[CH:26]=O.[NH3:30]>[N+]([O-])([O-])=O.[Ag+]>[CH3:23][O:24][CH:25]([O:28][CH3:29])[C:26]1[NH:30][C:2]([CH2:1][CH3:6])=[C:3]([C:10]([F:22])([F:21])[F:9])[N:5]=1参加物
6
実験手順
The same operation as in Example (36b) was performed using NCS (1.35 g, 10.1 mmol), silver nitrate (2.45 g, 14.4 mmol), 2,2,2-trifluoro-1-(2-ethyl-1,3-dithian-2-yl)ethanone obtained in Example (39b) (1.0 g, 4.09 mmol), dimethoxyacetaldehyde (5.76 M aqueous solution, 1.0 mL, 5.76 mmol) and 28% aqueous ammonia (4 mL). The resulting compound was used for the next reaction without purification.
後処理
- customThe resulting compound was used for the next reaction without purification
出典と根拠
- ORDレコード
- ord-ef9ba275c62b456e8ce8698492098cc5
- 出典データセット
- uspto-grants-2013_09
- 特許番号
- US08536197B2
関連ノート
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