Sodium Carbonate → HCID 12671198、化合物
反応式
Cl[C:2]1[N:7]2[N:8]=[CH:9][N:10]=[C:6]2[N:5]=[C:4]([CH3:11])[C:3]=1[CH2:12][CH2:13]Cl.[CH:15]([NH2:19])([CH2:17][CH3:18])[CH3:16].C(=O)([O-])[O-].[Na+].[Na+]>C(O)C>[CH:15]([N:19]1[C:2]2[N:7]3[N:8]=[CH:9][N:10]=[C:6]3[N:5]=[C:4]([CH3:11])[C:3]=2[CH2:12][CH2:13]1)([CH2:17][CH3:18])[CH3:16]参加物
5
実験手順
A mixture of 2.3g of 7-chloro-6-(2-chloroethyl)-5-methyl-s-triazolo[1,5-a]pyrimidine, 1g of sec-butylamine, 1.8g of sodium carbonate and 20 ml of ethanol was refluxed for 2 hours. The hot reaction mixture was then filtered and the filtrate was concentrated under reduced pressure.
後処理
- temperaturewas refluxed for 2 hours
- filtrationThe hot reaction mixture was then filtered
- concentrationthe filtrate was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-9b201f68a2ab49968ca8a5957d493227
- 出典データセット
- uspto-grants-1977_02
- 特許番号
- US04007189
反応ノート
読み込み中…