化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → 1-Methyl-s-triazolo[4,3-a]quinoxaline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | 2-Hydrazinoquinoxaline | HCID 289847 | — |
| 生成物 | 1-Methyl-s-triazolo[4,3-a]quinoxaline | HCID 21817404 | — |
反応手順
A 5 g. portion of 2-hydrazinoquinoxaline was stirred at reflux temperature in acetic acid for 3 hours. The reaction mixture was then cooled, and was evaporated to dryness under vacuum. The product was found to melt at 210°-12° C. without purification, and was identified as 1-methyl-s-triazolo[ 4,3-a]quinoxaline by NMR analysis and elemental microanalysis, the results of which follow.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04008322 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-4a363311389b443a82fd6b09271767e6 |
| 出典メモ | uspto-grants-1977_02 |