化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Hydroxide → N,N'-Heptamethylenebis(3,4-methylenedioxybenzamide)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 1,7-Heptanediamine | HCID 69533 | — |
| 反応物 | 1,3-Benzodioxole-5-carbonyl chloride | HCID 2734749 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | N,N'-Heptamethylenebis(3,4-methylenedioxybenzamide) | HCID 4132789 | — |
反応手順
m.p. 151°-152° C., 24.9 g., was prepared as in Example 1 using 3,4-methylenedioxybenzoyl chloride (prepared as in Example 6 using 30 g. of 3,4 -methylenedioxybenzoic acid) in 150 ml. of ethylene dichloride, 10.5 g. of 1,7-heptanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from ethanol using decolorizing charcoal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04009208 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-57bbe104ff3e4bda931143beac89bb8d |
| 出典メモ | uspto-grants-1977_02 |