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Methanol → 6-Methoxy-2-naphthylacetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | Methyl 6-methoxynaphthalene-2-acetate | HCID 90324 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 6-Methoxy-2-naphthylacetic acid | HCID 32176 | — |
反応手順
A mixture of 25 g. of methyl 6-methoxy-2-naphthylacetate, 15 g. of sodium carbonate, 200 ml. of methanol, and 25 ml. of water are stirred for 24 hours. The reaction mixture is then acidified with 200 ml. of 2 N hydrochloric acid and extracted with methylene chloride. The extracts are combined, washed with water, dried over sodium sulfate, and evaporated to yield 6-methoxy-2-naphthylacetic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04009197 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-3b933a6a881645fa95e6a20e77521c65 |
| 出典メモ | uspto-grants-1977_02 |