N,N-Dimethylallylamine → Allyl n-butoxymethyl dimethylammonium chloride

HRID 437030

反応式

HRID 437030 の反応式
[CH2:1]([O:5][CH2:6][Cl:7])[CH2:2][CH2:3][CH3:4].[CH2:8]([N:11]([CH3:13])[CH3:12])[CH:9]=[CH2:10]>C(OCC)(=O)C>[Cl-:7].[CH2:8]([N+:11]([CH2:6][O:5][CH2:1][CH2:2][CH2:3][CH3:4])([CH3:13])[CH3:12])[CH:9]=[CH2:10]

参加物

4

反応物 2

HCID 75082N,N-DimethylallylamineHCID 111053571-(Chloromethoxy)butane

生成物 1

HCID 21429949Allyl n-butoxymethyl dimethylammonium chloride

試薬・触媒・溶媒 1

HCID 8857Ethyl Acetate溶媒

実験手順

24.7 grams of chloromethyl butyl ether was added to 17 grams of allyl dimethylamine in 32 grams of ethyl acetate. The reaction was highly exothermic and two layers formed very rapidly. Stirring was continued at 25° C. for 24 hours, after which the solvent was removed by vacuum. Chloride analysis of the rather viscous liquid product indicated 91% of theoretical.

後処理

  1. customtwo layers formed very rapidly
  2. customafter which the solvent was removed by vacuum

出典と根拠

ORDレコード
ord-555e2f750b504c65a2b53b679bcae8c9
出典データセット
uspto-grants-1977_06
特許番号
US04029658

関連ノート

読み込み中…