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Methane → 2-(6-Carboxyhexyl)benzyl alcohol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methane | HCID 297 | — |
| 反応物 | Heptenoic acid | HCID 29373 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-(6-Carboxyhexyl)benzyl alcohol | HCID 53971444 | — |
反応手順
A solution of 2.30 g. of the above heptenoic acid in 100 ml. of ethanol is stirred with 5 g. of activated charcoal for 30 minutes and filtered. The filtrate is hydrogenated at atmospheric pressure in the presence of 143 mg. of platinum oxide. The solution is filtered, evaporated and recrystallized from toluene to yield 2-(6-carboxyhexyl)benzyl alcohol as white crystals having a melting point of 75°-77° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04032656 |
| 出典データセット | uspto-grants-1977_06 |
| ORD ID | ord-a434d3d6d1b8480e8bb79ac2a2025f06 |
| 出典メモ | uspto-grants-1977_06 |