HRID437987

反应详情

EQUATION

反应方程式

HRID 437987 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 2.30 g. of the above heptenoic acid in 100 ml. of ethanol is stirred with 5 g. of activated charcoal for 30 minutes and filtered. The filtrate is hydrogenated at atmospheric pressure in the presence of 143 mg. of platinum oxide. The solution is filtered, evaporated and recrystallized from toluene to yield 2-(6-carboxyhexyl)benzyl alcohol as white crystals having a melting point of 75°-77° C.

WORKUP

后处理

  1. filtrationfiltered
  2. filtrationThe solution is filtered
  3. customevaporated
  4. customrecrystallized from toluene