Thionyl Chloride → 1-(2-Methoxyphenyl)cyclopropane-1-carbonyl chloride

HRID 440500ノート

反応式

HRID 440500 の反応式
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1([C:12]([OH:14])=O)[CH2:11][CH2:10]1.S(Cl)([Cl:17])=O>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1([C:12]([Cl:17])=[O:14])[CH2:11][CH2:10]1

参加物

3

反応物 2

HCID 24386Thionyl ChlorideHCID 184000111-(2-Methoxyphenyl)cyclopropane-1-carboxylic acid

生成物 1

HCID 242737911-(2-Methoxyphenyl)cyclopropane-1-carbonyl chloride

実験手順

1-(2-methoxyphenyl)cyclopropane carboxylic acid (19 g) and thionyl chloride (30 ml) were heated under gentle reflux for 2 hours. The solvent was evaporated to yield 1-(2-methoxyphenyl)cyclopropane carbonyl chloride.

後処理

  1. temperatureunder gentle reflux for 2 hours
  2. customThe solvent was evaporated

出典と根拠

ORDレコード
ord-9bd963ed53c64b00944548ac86d2f391
出典データセット
uspto-grants-1996_05
特許番号
US05519034

反応ノート

読み込み中…