化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → 2,4-Bis(2-ethyl-hexylamino)-6-(4-camphylidenemethylene-anilino)-1,3,5-triazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 2-Ethylhexylamine | HCID 7719 | — |
| 反応物 | Sodium Acetate | HCID 517045 | — |
| 反応物 | 2-(4-Camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine | HCID 86749508 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2,4-Bis(2-ethyl-hexylamino)-6-(4-camphylidenemethylene-anilino)-1,3,5-triazine | HCID 86749507 | — |
反応手順
A reaction mixture comprising 33 g (0.26 mol) of 2-ethylhexylamine and 50 g (0.12 mol) of 2-(4-camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine in toluene is heated to 90° C. in the presence of sodium acetate. When the starting materials have reacted completely, the mixture is worked up. The product (95%) is a yellow viscous oil. UV (ethanol, c=1 mg/100 ml): λmax =345 nm, E=0.57.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05520906 |
| 出典データセット | uspto-grants-1996_05 |
| ORD ID | ord-421b47c7408749a68881a84dac61fe1d |
| 出典メモ | uspto-grants-1996_05 |