Thionyl Chloride → HCID 14985095、化合物
反応式
[CH2:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:18]=[CH:17][C:13]([C:14](O)=[O:15])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)[CH2:2][CH3:3].S(Cl)([Cl:21])=O>C(Cl)Cl>[CH2:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:18]=[CH:17][C:13]([C:14]([Cl:21])=[O:15])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)[CH2:2][CH3:3]参加物
4
実験手順
A mixture of 2.0 g of 4-(4-propylphenyl]benzoic acid and 30 ml of thionyl chloride is stirred at reflux for 45 minutes. The reaction mixture is evaporated in vacuo to a residue which is evaporated from carbon tetrachloride (2×50 ml) to give a residue which is dissolved in methylene chloride.
後処理
- temperatureat reflux for 45 minutes
- customThe reaction mixture is evaporated in vacuo to a residue which
- customis evaporated from carbon tetrachloride (2×50 ml)
- customto give a residue which
出典と根拠
- ORDレコード
- ord-0f9b4676d93549f48a698d43bfb3bfe9
- 出典データセット
- uspto-grants-1996_05
- 特許番号
- US05521173
反応ノート
読み込み中…