Trimethylamine → trimethyl-N-2-hydroxypropyl ammonium isodecanoate

反応式

[C:1]([OH:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([CH3:10])[CH3:9].[CH3:13][N:14]([CH3:16])[CH3:15].[CH2:17]1[O:20][CH:18]1[CH3:19]>>[C:1]([O-:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([CH3:9])[CH3:10].[CH3:13][N+:14]([CH3:16])([CH3:15])[CH2:17][CH:18]([OH:20])[CH3:19]

参加物

反応物 3

HCID 1146Trimethylamine

HCID 6378Propylene Oxide

HCID 1114708-Methylnonanoic acid

生成物 1

HCID 86734985trimethyl-N-2-hydroxypropyl ammonium isodecanoate

実験手順

Following the procedure set out in Example 7 above, isodecanoic acid was reacted with equal molar quantities each of trimethylamine and propylene oxide to obtain trimethyl-N-2-hydroxypropyl ammonium isodecanoate which structure was confirmed by NMR analysis as reported in Table 2. ##STR5##

出典と根拠

ORDレコード: ord-49a335560cff4b7b841ab4177db086ad
出典データセット: uspto-grants-1977_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04040992

反応ノート

読み込み中…