Sodium Carbonate → HCID 86626532、化合物

HRID 44155ノート

反応式

HRID 44155 の反応式
[C:1]([O:8][CH:9]1[CH:14]([CH:15]([CH3:17])[CH3:16])[CH2:13][CH2:12][CH:11]([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].C(=O)([O-])[O-].[Na+:23].[Na+]>C(O)C>[C:1]([O:8][CH:9]1[CH:14]([CH:15]([CH3:17])[CH3:16])[CH2:13][CH2:12][CH:11]([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].[Na+:23]

参加物

4

反応物 2

HCID 10340Sodium CarbonateHCID 186766644-{[5-Methyl-2-(propan-2-yl)cyclohexyl]oxy}-4-oxobutanoate2 回

生成物 1

HCID 86626532HCID 86626532、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

Monomenthyl succinate (0.5 g, 1.95 mmol) was dissolved in ethanol (6.3 ml). Sodium carbonate solution (0.207 g, 1.95 mmol in 10 ml DI H2O) was slowly added to the monomenthyl succinate solution at room temperature. The mixture was allowed to stir for 19 hours. Water and ethanol were removed by rotary evaporator at 50° C., followed by high vacuum line at 50° C. to give sodium monomenthyl succinate as a fine white powder.

後処理

  1. customWater and ethanol were removed by rotary evaporator at 50° C.
  2. customfollowed by high vacuum line at 50° C.

出典と根拠

ORDレコード
ord-505f1cbfab264109893122616f8a8555
出典データセット
uspto-grants-2013_09
特許番号
US08541401B2

反応ノート

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