Oxalyl chloride → 4-Bromo-2-methylbenzoyl chloride

HRID 442796ノート

反応式

HRID 442796 の反応式
[CH3:1][C:2]1[CH:10]=[C:9]([Br:11])[CH:8]=[CH:7][C:3]=1[C:4](O)=[O:5].C(Cl)(=O)C([Cl:15])=O>ClCCl>[CH3:1][C:2]1[CH:10]=[C:9]([Br:11])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:15])=[O:5]

参加物

4

反応物 2

HCID 65578Oxalyl chlorideHCID 995704-Bromo-2-methylbenzoic acid

生成物 1

HCID 128464834-Bromo-2-methylbenzoyl chloride

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

実験手順

2-Methyl-4-bromobenzoic acid (26.8 g) was treated with oxalyl chloride (16.3 ml) in dry dichloromethane (250 ml) and the product was isolated by the method described in Example 1 (i) to give 2-methyl-4-bromobenzoyl chloride as an oil.

後処理

  1. customthe product was isolated by the method

出典と根拠

ORDレコード
ord-624766a2ab14426a9eeb80230cdc4cbc
出典データセット
uspto-grants-1999_04
特許番号
US05891899

反応ノート

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