Isoprene → Isoprene butadiene
反応式
[CH2:1]=[CH:2][CH:3]=[CH2:4].[CH2:5]=[CH:6][C:7](=[CH2:9])[CH3:8].C([Li])CCC>CCCCCCC>[CH2:1]=[CH:2][CH:3]=[CH2:4].[CH2:5]=[CH:6][C:7](=[CH2:8])[CH3:9]参加物
5
反応条件
- 温度
- 50 °C
実験手順
In a reactor, a mixture of 57 g of 1,3-butadiene and 37 g of isoprene is added to a solution of 12.5 mmoles of butyllithium in 250 ml of n-heptane. The reaction mixture is stirred for 5 hours at 50° C., which results in a complete conversion of the monomers to a butadiene-isoprene copolymer having a butadiene content of 60% by weight and an average molecular weight by number of 5700.
出典と根拠
- ORDレコード
- ord-daee73f20a3c41f9971fe910bad41998
- 出典データセット
- uspto-grants-1981_04
- 特許番号
- US04264334
反応ノート
読み込み中…