Adipic Acid → 6-(2,3-Dichlorophenyl)-1,2,4-triazine-3,5-diamine;hexanedioate

HRID 449791

反応式

HRID 449791 の反応式
[CH:1]1[CH:6]=[C:5]([Cl:7])[C:4]([Cl:8])=[C:3]([C:9]2[N:14]=[N:13][C:12]([NH2:15])=[N:11][C:10]=2[NH2:16])[CH:2]=1.[C:17]([OH:26])(=[O:25])[CH2:18][CH2:19][CH2:20][CH2:21][C:22]([OH:24])=[O:23]>CO>[CH:1]1[CH:6]=[C:5]([Cl:7])[C:4]([Cl:8])=[C:3]([C:9]2[N:14]=[N:13][C:12]([NH2:15])=[N:11][C:10]=2[NH2:16])[CH:2]=1.[C:17]([O-:26])(=[O:25])[CH2:18][CH2:19][CH2:20][CH2:21][C:22]([O-:24])=[O:23]

参加物

4

反応物 2

HCID 196Adipic AcidHCID 3878Lamotrigine

生成物 1

HCID 866323226-(2,3-Dichlorophenyl)-1,2,4-triazine-3,5-diamine;hexanedioate

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

16 mg of lamotrigine was dissolved in 2 ml of methanol, 11 mg of adipic acid was added to the solution to form a single solution. The solution was then allowed to stand for several hours to effect the slow evaporation of solvent. The solids gathered were stored in screw cap vials for subsequent analysis.

後処理

  1. customto form a single solution
  2. waitto stand for several hours
  3. customthe slow evaporation of solvent
  4. customcap vials for subsequent analysis

出典と根拠

ORDレコード
ord-9374823017d143f1a784e1a60c0199c4
出典データセット
uspto-grants-2013_07
特許番号
US08486927B2

関連ノート

読み込み中…