化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 2,6-Dichloro-4-iodobenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 2,6-Dichloro-4-iodobenzoic acid | HCID 51341877 | — |
| 生成物 | 2,6-Dichloro-4-iodobenzoyl chloride | HCID 86648958 | 100% |
反応手順
A solution of 2,6-dichloro-4-iodobenzoic acid (65 mg, 0.21 mmol) in SOCl2 (3 mL) was heated to reflux under nitrogen atmosphere overnight and then cooled to room temperature. The reaction was conentrated under reduced pressure to afford 2,6-dichloro-4-iodobenzoyl chloride (70 mg, 100% yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08486950B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-4d56422000ae457ca41ed97b75cb9c61 |
| 出典メモ | uspto-grants-2013_07 |