Hydrogen Bromide → HCID 68449648、化合物
反応式
C[O:2][C:3]1[N:8]=[C:7]([CH:9]([NH2:11])[CH3:10])[CH:6]=[CH:5][CH:4]=1.[BrH:12]>>[BrH:12].[NH2:11][CH:9]([C:7]1[NH:8][C:3](=[O:2])[CH:4]=[CH:5][CH:6]=1)[CH3:10]参加物
3
反応条件
- 温度
- 80 °C
実験手順
To 1.6 g of 1-(6-methoxypyridin-2-yl)ethanamine was added 23.7 ml of a 47% aqueous hydrobromic acid solution, followed by stirring at 80° C. for 60 hours. After evaporating the solvent under reduced pressure, the residue was washed with diethyl ether to obtain 2.95 g of 6-(1-aminoethyl)pyridin-2(1H)-one hydrobromide as a pale brown solid.
後処理
- customAfter evaporating the solvent under reduced pressure
- washthe residue was washed with diethyl ether
出典と根拠
- ORDレコード
- ord-49d23ee7360046fdaa26e23472ea494c
- 出典データセット
- uspto-grants-2013_07
- 特許番号
- US08486970B2
反応ノート
読み込み中…