Hydrogen Bromide → Hydrogen Bromide
反応式
C[O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH:9]1[CH2:14][CH2:13][CH2:12][NH:11][CH2:10]1.Cl.[BrH:16]>>[BrH:16].[NH:11]1[CH2:12][CH2:13][CH2:14][CH:9]([C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[OH:2])[CH2:10]1参加物
5
実験手順
HBr was prepared by heating 3-(2-methoxyphenyl)piperidine.HCl (46 mg, 0.20 mmol) with 48% HBr in a microwave reactor at 120° C. for one hour. After evaporation, 61 mg of the title compound was obtained.
後処理
- customAfter evaporation
出典と根拠
- ORDレコード
- ord-11dfe9e2a9a2445087b4c1b5f281be3e
- 出典データセット
- uspto-grants-2013_07
- 特許番号
- US08492549B2
反応ノート
読み込み中…