化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → Ethyl 3-bromo-4-methoxyphenylacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 3-Bromo-4-methoxyphenylacetic acid | HCID 136615 | — |
| 触媒 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | Ethyl 3-bromo-4-methoxyphenylacetate | HCID 57419861 | — |
反応手順
A solution of 3-bromo-4-methoxyphenylacetic acid (4.1 g, 16.7 mmol) and concentrated hydrogen chloride (2 drops) in EtOH (100 mL) were stirred at 80° C. for 3 days. After cooling to room temperature, the mixture was concentrated to dryness to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08497381B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-40154bfaaa5f406ca5094da0897e0562 |
| 出典メモ | uspto-grants-2013_07 |