1-Dodecanol → Lactic Acid
反応式
[C:1]([O-:6])(=[O:5])[CH:2]([CH3:4])[OH:3].[NH4+:7].C(O)CCCCCCCCCCC>>[C:1]([O-:6])(=[O:5])[CH:2]([CH3:4])[OH:3].[NH4+:7].[C:1]([OH:6])(=[O:5])[CH:2]([CH3:4])[OH:3]参加物
4
実験手順
The procedure described in Example 1 was followed except that the reaction solution consisted of 30 g of a 70% solution of ammonium lactate and 70 g dodecanol. The reaction mixture was heated for 1.5 hours at 105–110° C. and a reduced pressure of 1.1–2.2 mm Hg, resulting in a conversion of about 88% from ammonium lactate to lactic acid. Some of the dodecanol also reacted with lactic acid to form an ester. The conversion from ammonium lactate to lactic acid plus lactic acid ester was about 96%.
後処理
- temperatureThe reaction mixture was heated for 1.5 hours at 105–110° C.
出典と根拠
- ORDレコード
- ord-7ff503876ac742019720b10ecf3c1178
- 出典データセット
- uspto-grants-2007_03
- 特許番号
- US07186856B2
反応ノート
読み込み中…