関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Methyl 2-(2-nitro-4-(trifluoromethyl)phenyl)acetate | HCID 83569 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 生成物 | 6-Trifluoromethyloxindole | HCID 608487 | — |
反応手順
Methyl 2-nitro-4-trifluoromethylphenylacetate (26 mg) was hydrogenated over 10% palladium on carbon and then heated at 100° C. for 3 hours. The catalyst was removed by filtration and the solvent evaporated to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07189721B2 |
|---|
| 出典データセット | uspto-grants-2007_03 |
|---|
| ORD ID | ord-8297bf6395c54394842ec4283eb5610d |
|---|
| 出典メモ | uspto-grants-2007_03 |
|---|
