HCID 18443682、化合物 → 4-(Benzyloxy)-2-chlorobenzaldehyde
反応式
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][OH:16])=[C:11]([Cl:17])[CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>ClCCl.O=[Mn]=O>[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([CH:15]=[O:16])=[C:11]([Cl:17])[CH:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1参加物
4
実験手順
To a solution of (4-Benzyloxy-2-chloro-phenyl)-methanol in dichloromethane, MnO2 (10 eq) were added and the mixture reaction stirred overnight. Filtered through a pad of celite and purified by chromatography in silica gel to give the title product.
後処理
- customthe mixture reaction
- filtrationFiltered through a pad of celite
- custompurified by chromatography in silica gel
出典と根拠
- ORDレコード
- ord-4d2a72e663aa4d1c8863e6081abd266f
- 出典データセット
- uspto-grants-2007_03
- 特許番号
- US07192982B2
反応ノート
読み込み中…