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HRID 461152作成日：2026年10月26日

N,N'-Diethylthiourea → 3-Ethyl-2-ethylimino-4-(4-bromo-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride

https://huagongshe.com/reaction/461152

反応式

関与物質

役割名称HCID仕込み量
反応物N,N'-DiethylthioureaHCID 2735009—
反応物4'-Bromo-3'-sulfamoyl-2-chloroacetophenoneHCID 22760605—
生成物3-Ethyl-2-ethylimino-4-(4-bromo-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochlorideHCID 22760569—

反応手順

4.6 g of 4'-bromo-3'-sulfamoyl-2-chloroacetophenone and 1.8 g of ground 1,3-diethylthiourea were reacted and worked up according to the prescription given in Example 12. Colorless solid body, decomposition beginning at 103° C, C=N 1615 cm-1.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04061761
出典データセットuspto-grants-1977_12
ORD IDord-81597a29f4e242539630fe9460ef98a4
出典メモuspto-grants-1977_12