Methyl iodide → HCID 22768153、化合物

反応式

[CH2:1]([N:3]([CH2:16][CH2:17][CH2:18][CH3:19])[C:4]([NH:6][C:7]1[CH:11]=[C:10]([C:12]([CH3:15])([CH3:14])[CH3:13])[O:9][N:8]=1)=[O:5])[CH3:2].[CH3:20]I>>[CH2:1]([N:3]([CH2:16][CH2:17][CH2:18][CH3:19])[C:4]([N:6]([CH3:20])[C:7]1[CH:11]=[C:10]([C:12]([CH3:13])([CH3:15])[CH3:14])[O:9][N:8]=1)=[O:5])[CH3:2]

参加物

反応物 2

HCID 6328Methyl iodide

HCID 22768165N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N-ethylurea

生成物 1

HCID 22768153HCID 22768153、化合物

実験手順

The reaction is effected as in Example 171 by using 1-ethyl-1-butyl-3-(5-t-butyl-3-isoxazolyl)urea and methyl iodide to give 1-ethyl-1-butyl-3-methyl-3-(5-t-butyl-3-isoxazolyl)urea as an oil boiling at 140° to 145° C (bath temperature)/0.67 mm Hg.

出典と根拠

ORDレコード: ord-6d9ecf95f6ae4d3e9c5298a9e69558d6
出典データセット: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04062861

反応ノート

読み込み中…