Di-sodium 2,5-dichloroterephthalate → 1,4-Benzenedicarboxylic acid, 2,5-dichloro-

HRID 462038

反応式

HRID 462038 の反応式
[Cl:1][C:2]1[CH:10]=[C:9]([C:11]([O-:13])=[O:12])[C:8]([Cl:14])=[CH:7][C:3]=1[C:4]([O-:6])=[O:5].[Na+].[Na+]>[N+]([O-])([O-])=O.[Ag+]>[Cl:1][C:2]1[CH:10]=[C:9]([C:11]([OH:13])=[O:12])[C:8]([Cl:14])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5]

参加物

3

反応物 1

HCID 131710986Di-sodium 2,5-dichloroterephthalate

生成物 1

HCID 837391,4-Benzenedicarboxylic acid, 2,5-dichloro-

試薬・触媒・溶媒 1

HCID 24470Silver Nitrate触媒

実験手順

The di-silver salt of 2,5-dichloroterephthalic acid was prepared in quantitative yield from an aqueous solution of 1 mole di-sodium 2,5-dichloroterephthalate added to an aqueous solution of 2 moles of silver nitrate, by filtering, washing, and drying. The salt decomposes at 298° C.

後処理

  1. filtrationby filtering
  2. washwashing
  3. customdrying
  4. customdecomposes at 298° C.

出典と根拠

ORDレコード
ord-0e6f736c673d434fa8668f74720c40c7
出典データセット
uspto-grants-1977_12
特許番号
US04065442

関連ノート

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